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Standard Test Method for Acid and Base Number by Color-Indicator Titration (Includes all amendments And changes 2/26/2016).
Automaticky preložený názov:
Štandardná skúšobná metóda pre Acid a Base Number by Color - Ukazovateľ titrácia
NORMA vydaná dňa 1.12.2014
Označenie normy: ASTM D974-14e1
Poznámka: NEPLATNÁ
Dátum vydania normy: 1.12.2014
Kód tovaru: NS-613025
Počet strán: 7
Približná hmotnosť: 21 g (0.05 libier)
Krajina: Americká technická norma
Kategória: Technické normy ASTM
Ropné produkty všeobecně
Maziva, průmyslové oleje a odpovídající výrobky
Keywords:
acid number, base number, color indication titration, petroleum products,, ICS Number Code 75.080 (Petroleum products in general), 75.100 (Lubricants, industrial oils and related products)
Significance and Use | ||||||||||
5.1 New and used petroleum products can contain basic or acidic constituents that are present as additives or as degradation products formed during service, such as oxidation products. The relative amount of these materials can be determined by titrating with acids or bases. This number, whether expressed as 5.2 Since a variety of oxidation products contribute to the acid number and the organic acids vary widely in corrosive properties, the test cannot be used to predict corrosiveness of an oil under service conditions. No general correlation is known between acid number and the corrosive tendency of oils toward metals. Compounded engine oils can and usually do have both acid and base numbers in this test method. |
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1. Scope | ||||||||||
1.1 This test method covers the determination of acidic or basic constituents (Note 1) in petroleum products2 and lubricants soluble or nearly soluble in mixtures of toluene and isopropyl alcohol. It is applicable for the determination of acids or bases whose dissociation constants in water are larger than 10−9; extremely weak acids or bases whose dissociation constants are smaller than 10−9 do not interfere. Salts react if their hydrolysis constants are larger than 10−9. Note 1: In new and used oils, the constituents considered to
have acidic characteristics include organic and inorganic acids,
esters, phenolic compounds, lactones, resins, salts of heavy
metals, and addition agents such as inhibitors and detergents.
Similarly, constituents considered to have basic properties include
organic and inorganic bases, amino compounds, salts of weak acids
(soaps), basic salts of polyacidic bases, salts of heavy metals,
and addition agents such as inhibitors and detergents.
Note 2: This test method is not suitable for measuring the
basic constituents of many basic additive-type lubricating oils.
Test Method D4739 can be used
for this purpose.
1.2 This test method can be used to indicate relative changes that occur in an oil during use under oxidizing conditions. Although the titration is made under definite equilibrium conditions, the method does not measure an absolute acidic or basic property that can be used to predict performance of an oil under service conditions. No general relationship between bearing corrosion and acid or base numbers is known. Note 3: Oils, such as many cutting oils, rustproofing oils,
and similar compounded oils, or excessively dark-colored oils, that
cannot be analyzed for acid number by this test method due to
obscurity of the color-indicator end point, can be analyzed by Test
Method D664. The acid numbers
obtained by this color-indicator test method need not be
numerically the same as those obtained by Test Method D664, the base numbers obtained by this
color indicator test method need not be numerically the same as
those obtained by Test Method D4739, but they are generally of the same
order of magnitude.
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. |
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2. Referenced Documents | ||||||||||
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