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Standard Test Method for Condition Monitoring of Nitration in In-Service Petroleum and Hydrocarbon-Based Lubricants by Trend Analysis Using Fourier Transform Infrared (FT-IR) Spectrometry
NORMA vydaná dňa 1.12.2021
Označenie normy: ASTM D7624-21
Dátum vydania normy: 1.12.2021
Kód tovaru: NS-1047544
Počet strán: 5
Približná hmotnosť: 15 g (0.03 libier)
Krajina: Americká technická norma
Kategória: Technické normy ASTM
condition monitoring, differential trend analysis, direct trend analysis, Fourier transform infrared, FT-IR, hydrocarbon-based lubricants, infrared, in-service petroleum lubricants, IR, lubricants, nitration, oils,, ICS Number Code 75.100 (Lubricants, industrial oils and related products),75.160.20 (Liquid fuels)
|Significance and Use|
5.1There is a wide variety of nitration compounds that may be produced and accumulate when oils react with gaseous nitrates formed during the engine combustion process. These nitration products may increase the viscosity, acidity and insolubles in the oil, which may lead to ring sticking and filter plugging. Monitoring of nitration products is therefore an important parameter in determining overall machinery health and should be considered in conjunction with data from other tests such as atomic emission (AE) and atomic absorption (AA) spectroscopy for wear metal analysis (Test Method ), physical property tests (Test Methods and ), and other FT-IR oil analysis methods for oxidation (Test Method ), sulfate by-products (Test Method ), and additive depletion (Test Method ), which also assess elements of the oils condition 1.1This test method covers monitoring nitration in gasoline and natural gas engine oils as well as in other types of lubricants where nitration by-products may form due to the combustion process or other routes of formation of nitration compounds.
1.2This test method uses FT-IR spectroscopy for monitoring build-up of nitration by-products in in-service petroleum and hydrocarbon-based lubricants as a result of normal machinery operation. Nitration levels in gasoline and natural gas engine oils rise as combustion by-products react with the oil as a result of exhaust gas recirculation or a blow-by. This test method is designed as a fast, simple spectroscopic check for monitoring of nitration in in-service petroleum and hydrocarbon-based lubricants with the objective of helping diagnose the operational condition of the machine based on measuring the level of nitration in the oil.
1.3Acquisition of FT-IR spectral data for measuring nitration in in-service oil and lubricant samples is described in Practice . In this test method, measurement and data interpretation parameters for nitration using both direct trend analysis and differential (spectral subtraction) trend analysis are presented.
1.4This test method is based on trending of spectral changes associated with nitration in in-service petroleum and hydrocarbon-based lubricants. For direct trend analysis, values are recorded directly from absorption spectra and reported in units of 100*absorbance per 0.1mm pathlength (or equivalently absorbance units per centimetre). For differential trend analysis, values are recorded from the differential spectra (spectrum obtained by subtraction of the spectrum of the reference oil from that of the in-service oil) and reported in units of 100*absorbance per 0.1 mm pathlength (or equivalently absorbance units per centimetre). Warnings or alarm limits can be set on the basis of a fixed maximum value for a single measurement or, alternatively, can be based on a rate of change of the response measured Note 1:It is not the intent of this test method to establish or recommend normal, cautionary, warning or alert limits for any machinery. Such limits should be established in conjunction with advice and guidance from the machinery manufacturer and maintenance group.
1.5This test method is for petroleum and hydrocarbon-based lubricants and is not applicable for ester-based oils, including polyol esters or phosphate esters.
1.6The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.6.1ExceptionThe unit for wave numbers is cm-1.
1.7This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.8This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
|2. Referenced Documents|
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