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Standard Practice for Performing Detection and Quantitation Estimation and Data Assessment Utilizing DQCALC Software, based on ASTM Practices D6091 and D6512 of Committee D19 on Water (Includes all amendments and changes 12/29/2016).
NORMA vydaná dňa 15.12.2016
Označenie normy: ASTM D7510-10(2016)e1
Dátum vydania normy: 15.12.2016
Kód tovaru: NS-672817
Počet strán: 2
Približná hmotnosť: 6 g (0.01 libier)
Krajina: Americká technická norma
Kategória: Technické normy ASTM
Keywords:
detection, DQCALC, IDE, IQE, quantitation,, ICS Number Code 17.020 (Metrology and measurement in general)
Adjunct to D7510 Standard Practice for Performing Detection and Quantitation Estimation and Data Assessment Utilizing DQCALC Software, based on ASTM Practices D6091 and D6512 of Committee D19 on Water and D2777 Standard Practice for Determination of Preci
Vybraný formát:1. Scope | ||||||||
1.1 This software was developed to automate calculations within three ASTM standards: Practices D2777 (outlier removal section), D6091, and D6512. 1.2 The program calculates detection estimates (DE) and quantitation estimates (QE) for the constant, straight-line, exponential, and hybrid (Rocke-Lorenzato) models of the variation of [inter or intra] laboratory standard deviation (ILSD) with concentration. Calculations are shown in the DE_QE worksheet and results are shown in the DLs & QLs worksheet. Several plots are generated showing how well each model fits the data. The least complex model to fit the data with adequate confidence must be used by the ASTM standards. Note 1: Modeling techniques automated in this practice and
with this software have been shown to work well with most data
sets. Users of this software are cautioned that with some, rare
data sets, anomalous results may be obtained, and manual forcing of
a different model may be required. It has been noted that for some
data sets when an exponential model is selected, there may be a
lack of convergence on a result or there may be a convergence on
two separate results.
1.3 Users of DQCALC should refer to Practices D2777, D6091, and D6512 for the specifics of the scope and application of the Practices. 1.4 The IDE Practice (D6091) and the IQE Practice (D6512) are concerned with estimates of limits of detection and limits of quantitation based on inter-laboratory data. DQCALC may also be employed to calculate detection and quantitation estimates based on single laboratory data. 1.5 The DQCALC Software consists of a
Microsoft Excel
Standard Practice for Determination of
Precision and Bias of Applicable Test Methods of Committee D19 on
Water Adjunct to D7510 Standard Practice for
Performing Detection and Quantitation Estimation and Data
Assessment Utilizing DQCALC Software, based on ASTM Practices D6091
and D6512 of Committee D19 on Water and D2777 Standard Practice for
Determination of Preci Adjunct to D7510 Standard Practice for
Performing Detection and Quantitation Estimation and Data
Assessment Utilizing DQCALC Software, based on ASTM Practices D6091
and D6512 of Committee D19 on Water and D2777 Standard Practice for
Determination of Preci DQCALC Microsoft Excel-based software for
the Inter-laboratory Quantitation Estimate (IQE) |
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