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Standard Test Method for Total Cyanide in Water by Micro Distillation followed by Flow Injection Analysis with Gas Diffusion Separation and Amperometric Detection
NORMA vydaná dňa 1.8.2020
Označenie normy: ASTM D7284-20
Dátum vydania normy: 1.8.2020
Kód tovaru: NS-1001400
Počet strán: 7
Približná hmotnosť: 21 g (0.05 libier)
Krajina: Americká technická norma
Kategória: Technické normy ASTM
Keywords:
amperometry, cyanide, distillation, flow injection analysis, gas diffusion membrane, total cyanide,, ICS Number Code 13.060.50 (Examination of water for chemical substances)
Significance and Use | ||||||||||||||||||||
5.1 Cyanide and hydrogen cyanide are highly toxic. Regulations have been established to require the monitoring of cyanide in industrial and domestic wastes and surface waters.5.2 This test method is applicable for natural waters, industrial wastewaters and effluents. |
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1. Scope | ||||||||||||||||||||
1.1 This test method is used to determine the concentration of total cyanide in an aqueous wastewater or effluent. This test method detects the cyanides that are free (HCN and CN–) and strong-metal-cyanide complexes that dissociate and release free cyanide when refluxed under strongly acidic conditions. 1.2 This test method may not be applicable to process solutions from precious metals mining operations. 1.3 This procedure is applicable over a range of approximately 2 to 500 μg/L (parts per billion) total cyanide. Higher concentrations can be measured with sample dilution or lower injection volume. 1.4 The determinative step of this test method utilizes flow injection with amperometric detection based on Test Method D6888. Prior to analysis, samples must be distilled with a micro-distillation apparatus described in this test method or with a suitable cyanide distillation apparatus specified in Test Methods D2036. 1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. |
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2. Referenced Documents | ||||||||||||||||||||
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