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Standard Test Method for Analysis of Engine Coolant for Chloride and Other Anions by Ion Chromatography (Includes all amendments And changes 6/5/2015).
Automaticky preložený názov:
Štandardná skúšobná metóda pre analýzu chladiacej kvapaliny motora na chloridy a ďalšie anióny iónovou chromatografiou
NORMA vydaná dňa 1.3.2009
Označenie normy: ASTM D5827-09e1
Poznámka: NEPLATNÁ
Dátum vydania normy: 1.3.2009
Kód tovaru: NS-32705
Počet strán: 6
Približná hmotnosť: 18 g (0.04 libier)
Krajina: Americká technická norma
Kategória: Technické normy ASTM
Keywords:
chloride, chromatography methods, engine coolant, ion chromatography, Chloride analysis--engine coolants, Engine coolants/concentrates, Ion chromatography (IC), Chloride analysis--engine coolants, Engine coolants/concentrates, Ion chromatography (IC), ICS Number Code 71.100.45 (Refrigerants and antifreezes)
Significance and Use | ||||||||||||||||
This test method provides for the qualitative and quantitative determination of common anions in engine coolant in the milligrams per litre to low percent range and requires only a few millilitres or microlitres of sample per test, with results available in less than 30 min. Acceptable levels of chloride and other anions vary with manufacturer's blending specifications and applicable ASTM minimum or maximum specifications. |
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1. Scope | ||||||||||||||||
1.1 This test method covers the chemical analysis of engine coolant for chloride ion by high-performance ion chromatography (HPIC). Several other common anions found in engine coolant can be determined in one chromatographic analysis by this test method. 1.2 This test method is applicable to both new and used engine coolant. 1.3 Coelution of other ions may cause interferences for any of the listed anions. In the case of unfamiliar formulations, identification verification should be performed by either or both fortification and dilution of the sample matrix with the anions of interest. 1.4 Analysis can be performed directly by this test method without pretreatment, other than dilution, as required by the linear ranges of the equipment. Table 1 indicates several applicable anions and approximate detection limits. 1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to its use. TABLE 1 Analytes and Minimum Detection Limits
A Determined using 100-μL sample volume. Sample diluted 99 + 1 (v/v) with chromatographic eluant 30-μS/cm full scale, suppressed conductivity detection. Dionex AS4ASC column with AG4ASC guard columns. Other systems will require MDL determinations using chosen dilution factors, eluants, columns, and detector. |
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2. Referenced Documents | ||||||||||||||||
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