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ASTM D5185-18
Standard Test Method for Multielement Determination of Used and Unused Lubricating Oils and Base Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
NORMA vydaná dňa 1.4.2018
Informácie o norme:
Označenie normy: ASTM D5185-18
Dátum vydania normy: 1.4.2018
Kód tovaru: NS-818711
Počet strán: 9
Približná hmotnosť: 27 g (0.06 libier)
Krajina: Americká technická norma
Kategória: Technické normy ASTM
Kategórie - podobné normy:
Fyzikálně chemické analytické metody
Maziva, průmyslové oleje a odpovídající výrobky
Anotácia textu normy ASTM D5185-18 :
Keywords:
additive-elements, aluminum, barium, boron, calcium, chromium, copper, emission-spectrometry, ICP, inductively coupled plasma atomic emission spectrometry, iron, lead, lubricating oils, magnesium, manganese, molybdenum, nickel, phosphorous, potassium, silicon, silver, sodium, sulfur, tin, titanium, vanadium, wear metals, zinc,, ICS Number Code 71.040.50 (Physicochemical methods of analysis), 75.100 (Lubricants, industrial oils and related products)
Doplňujúce informácie
| Significance and Use | ||||||||||||||||||
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5.1 This test method covers the rapid determination of 22 elements in used and unused lubricating oils and base oils, and it provides rapid screening of used oils for indications of wear. Test times approximate a few minutes per test specimen, and detectability for most elements is in the low mg/kg range. In addition, this test method covers a wide variety of metals in virgin and re-refined base oils. Twenty-two elements can be determined rapidly, with test times approximating several minutes per test specimen. 5.2 When the predominant source of additive elements in used lubricating oils is the additive package, significant differences between the concentrations of the additive elements and their respective specifications can indicate that the incorrect oil is being used. The concentrations of wear metals can be indicative of abnormal wear if there are baseline concentration data for comparison. A marked increase in boron, sodium, or potassium levels can be indicative of contamination as a result of coolant leakage in the equipment. This test method can be used to monitor equipment condition and define when corrective actions are needed. 5.2.1 The significance of metal analysis in used lubricating oils is tabulated in Table 4. 5.3 The concentrations of metals in re-refined base oils can be indicative of the efficiency of the re-refining process. This test method can be used to determine if the base oil meets specifications with respect to metal content. |
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| 1. Scope | ||||||||||||||||||
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1.1 This test method covers the determination of additive elements, wear metals, and contaminants in used and unused lubricating oils and base oils by inductively coupled plasma atomic emission spectrometry (ICP-AES). The specific elements are listed in Table 1. 1.2 This test method covers the
determination of selected elements, listed in Table 1, in re-refined and virgin base
oils.
1.3 For analysis of any element using wavelengths below 190 nm, a vacuum or inert-gas optical path is required. The determination of sodium and potassium is not possible on some instruments having a limited spectral range. 1.4 This test method uses oil-soluble metals for calibration and does not purport to quantitatively determine insoluble particulates. Analytical results are particle size dependent, and low results are obtained for particles larger than a few micrometers.2 1.5 Elements present at concentrations above the upper limit of the calibration curves can be determined with additional, appropriate dilutions and with no degradation of precision. 1.6 For elements other than calcium, sulfur, and zinc, the low limits listed in Table 2 and Table 3 were estimated to be ten times the repeatability standard deviation. For calcium, sulfur, and zinc, the low limits represent the lowest concentrations tested in the interlaboratory study. 1.7 The values stated in SI units are to
be regarded as standard. No other units of measurement are included
in this standard.
1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. |
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| 2. Referenced Documents | ||||||||||||||||||
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