ASTM D4543-19

4.1 The dimensional, shape, and surface tolerances of rock core test specimens are important for determining rock properties of intact specimens. This is especially true for strong rocks, greater than 7250 psi (50 MPa) and for rock specimens that will be tested in stiff testing load frames without a spherical seat where non-uniform loading could occur. Dimensional and surface tolerance checks are required in the test methods listed in Section 2.1. To simplify test procedures in laboratories, the parts of those procedures that are common to the test methods in Section 2.1 are given in this standard.

4.2 This procedure is applicable to all the standards listed in Section 2.1; however, specimens for Test Method D2936 do not need to be machined or to meet the specified tolerances for flatness and parallelism.

4.3 The moisture condition of the specimen at the time of the sample preparation can have a significant effect upon the strength and deformation characteristics of the rock. Good practice generally dictates that laboratory tests be made upon a specimens’ representative of field conditions. Thus, it follows that the field moisture condition of the specimen should be preserved until the time of the test. In some instances, however, there may be reasons for testing specimens at other moisture contents, from saturation to dry. In any case, the moisture content of the test specimen should be tailored to the problem at hand.

4.4 Excess moisture will affect the adhesion of resistance strain gages, if used, and the accuracy of their performance. Adhesives used to bond the rock to steel end caps and fixtures for attaching specimens to actuators and crosshead of the load frame in the direct tension test (D2936) will also be affected adversely by excess moisture.

1.1 These practices specify procedures for preparing rock test specimen of rock core from drill core obtained in the field or from block samples for strength and deformation testing and for determining the conformance of the test specimen dimensions with tolerances established by this practice. Cubical, rectangular, or other shapes are not covered by this practice. However, some of the information contained within this practice and in standard Test Method C170 may still be of use to preparing other test specimen shapes.

1.2 Rock is a complex engineering material that can vary greatly as a function of lithology, stress history, weathering, moisture content and chemistry, and other natural geologic processes. As such, it is not always possible to obtain or prepare rock core specimens that satisfy the desirable tolerances given in this practice. Most commonly, this situation presents itself with weaker, more porous, and poorly cemented rock types and rock types containing significant or weak (or both) structural features. For rock types which are difficult to prepare, all reasonable efforts should be made to prepare a specimen in accordance with this practice and for the intended test procedure. However, when it has been determined by trial and error that this is not possible, prepare the rock specimen to the closest tolerances practicable and consider this to be the best effort (Note 1) and report it as such and if allowable or necessary for the intended test, capping the ends of the specimen as discussed in this practice is permitted.

1.3 This practices covers some, but not all of the curatorial issues that should be implemented. For curatorial issues that should be followed before and during specimen preparation refer to Practices D5079 and to the specific test standards in 2.1 for which the specimens are being prepared.

1.4 This practice also prescribes tolerance checks on the length-to-diameter ratio, straightness of the elements on the cylindrical surface, the flatness of the end bearing surfaces, and the perpendicularity of the end surfaces with the axis of the core.

1.5 The requirement for specifying the moisture condition and volume of the test specimen is also stated. However, the requirements in the specific test standards in 2.1 should be followed too.

1.6 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026, unless superseded by this standard.

1.7 Units—The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard. Add if appropriate, “Reporting of test results in units other than inch-pound shall not be regarded as nonconformance with this standard.”

1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.9 These practices offer a set of instructions for performing one or more specific operations. This document cannot replace education or experience and should be used in conjunction with professional judgement. Not all aspects of this practice may be applicable in all circumstances. This ASTM standard is not intended to represent or replace the standard of care by which the adequacy of a given professional service must be judged, nor should this document be applied without consideration of a project's many unique aspects. The word “standard” in the title of this document means only that the document has been approved through the ASTM consensus process.

1.10 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.