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Standard Test Method for Water in Paints and Paint Materials by Karl Fischer Method (Includes all amendments And changes 6/12/2015).
Automaticky preložený názov:
Štandardná skúšobná metóda pre vodu v Farby a náterové hmoty Karl Fischer
NORMA vydaná dňa 1.2.2008
Označenie normy: ASTM D4017-02(2008)e1
Poznámka: NEPLATNÁ
Dátum vydania normy: 1.2.2008
Kód tovaru: NS-25738
Počet strán: 8
Približná hmotnosť: 24 g (0.05 libier)
Krajina: Americká technická norma
Kategória: Technické normy ASTM
Keywords:
Karl Fischer reagent method, moisture content, water content, Karl Fischer reagent method--water content, Moisture analysis--paints/related coatings/materials, Solvents--paints/related coatings/materials, Water content--paints/related coatings/materials, Latex paints, Monomers, Pyridine, Resins, Solventborne paints/coatings, ICS Number Code 87.040 (Paints and varnishes)
Significance and Use | ||||||||
Control of water content is often important in controlling the performance of paint and paint ingredients, and it is critical in controlling volatile organic compound (VOC) content. Paint materials are often insoluble in common Karl Fischer solvents such as methanol. Pyridine has been found to be a nearly universal solvent for these materials; however, the Karl Fischer reaction is too slow in that solvent at room temperature. To speed it up, 1-ethylpiperidine is added at 5 % as a buffer, or “catalyst.” For nonpyridine-based reagents, a number of different solvent systems are available to increase solubility and to minimize interferences from ketones and aldehydes. |
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1. Scope | ||||||||
1.1 This test method is applicable to all paints and paint materials, including resins, monomers, and solvents, with the exception of aldehydes and certain active metals, metal oxides, and metal hydroxides. While the evaluation was limited to pigmented products containing amounts of water in the 30 to 70 % range, there is reason to believe that higher and lower concentrations can be determined by this test method. 1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific hazard statements are given in Section 7. |
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2. Referenced Documents | ||||||||
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