ASTM C633-01

This test method is recommended for quality control, acceptance testing; or it may help to develop or qualify a thermal spray operator’ equipment and procedure or to aid in developing thermal spray coatings with improved adhesion and integrity.

This test method is useful for comparing adhesion or cohesion strengths of coatings of similar types of thermal spray materials. The test should not be considered to provide an intrinsic value for direct use in making calculations, such as to determine if a coating will withstand specific environmental stresses. Because of residual stresses in thermal spray coatings, actual strength depends upon the shape of the particular coated part. Also, in use, a coating may be stressed in a more complex manner than is practical for a standard test.

1.1 This test method covers the determination of the degree of adhesion (bonding strength) of a coating to a substrate or the cohesion strength of the coating in a tension normal to the surface. The test consists of coating one face of a substrate fixture, bonding this coating to the face of a loading fixture, and subjecting this assembly of coating and fixtures to a tensile load normal to the plane of the coating. It is adapted particularly for testing coatings applied by thermal spray, which is defined to include the combustion flame, plasma arc, two-wire arc, high-velocity oxygen fuel, and detonation processes for spraying feedstock, which may be in the form of, wire, rod, or powder.

Note 1--Thermal spray coating materials include ceramics, such as metal oxides or carbides, and metals. In some cases, a coating is formed of different spray materials, such as an oxide layer sprayed onto a sprayed metal-bonding layer. The substrate generally is a metal, but may be a ceramic, such as an oxide or graphite.

1.2 Usually this test method is performed at ambient temperature. Higher temperature testing is restricted by the need for a suitable adhesive bonding agent. For certain fundamental investigations, it is suggested that very low (cryogenic) temperature be used.

1.3 This test method is limited to testing thermal spray coatings that can be applied in thickness greater than 0.015 in. (0.38 mm). The limitation is imposed because an adhesive bonding agent is used in the test. Those bonding agents established so far for this method tend to penetrate thermal spray coatings and may invalidate results unless the coatings are thick enough to prevent penetration through the coating. Further development may establish that thin layers of certain types of especially dense coatings may be tested satisfactorily. Alternatively, new adhesive bonding agents that would allow reduction of the minimum thickness limitation may become available.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health limitations prior to use.