ASTM A1033-10(2015)

5.1 This practice is used to provide steel phase transformation data required for use in numerical models for the prediction of microstructures, properties, and distortion during steel manufacturing, forging, casting, heat treatment, and welding. Alternatively, the practice provides end users of steel and fabricated steel products the phase transformation data required for selecting steel grades for a given application by determining the microstructure resulting from a prescribed thermal cycle.

5.2 It should be recognized that thermal and transformation strains, which develop in steels during thermal cycling, are sensitive to chemical composition. Thus, anisotropy in chemical composition can result in variability in strain, and can affect the results of strain determinations, especially determination of volumetric strain. Strains determined during cooling are sensitive to the grain size of austenite, which is determined by the heating cycle. The most consistent results are obtained when austenite grain size is maintained between ASTM grain sizes of 5 to 8. Finally, the eutectoid carbon content is defined as 0.8 % for carbon steels. Additions of alloying elements can change this value, along with Ac₁ and Ac₃ temperatures. Heating cycles need to be employed, as described below, to ensure complete formation of austenite preceding strain measurements during cooling.

1.1 This practice covers the determination of hypoeutectoid steel phase transformation behavior by using high-speed dilatometry techniques for measuring linear dimensional change as a function of time and temperature, and reporting the results as linear strain in either a numerical or graphical format.

1.2 The practice is applicable to high-speed dilatometry equipment capable of programmable thermal profiles and with digital data storage and output capability.

1.3 This practice is applicable to the determination of steel phase transformation behavior under both isothermal and continuous cooling conditions.

1.4 This practice includes requirements for obtaining metallographic information to be used as a supplement to the dilatometry measurements.

1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.