ASTM C1368-10(2017)

4.1 For many structural ceramic components in service, their use is often limited by lifetimes that are controlled by a process of SCG. This test method provides the empirical parameters for appraising the relative SCG susceptibility of ceramic materials under specified environments. Furthermore, this test method may establish the influences of processing variables and composition on SCG as well as on strength behavior of newly developed or existing materials, thus allowing tailoring and optimizing material processing for further modification. In summary, this test method may be used for material development, quality control, characterization, and limited design data generation purposes. The conventional analysis of constant stress-rate testing is based on a number of critical assumptions, the most important of which are listed in the next paragraphs.

4.2 The flexural stress computation for the rectangular beam test specimens or the equibiaxial disk flexure test specimens is based on simple beam theory, with the assumptions that the material is isotropic and homogeneous, the moduli of elasticity in tension and compression are identical, and the material is linearly elastic. The average grain size should be no greater than one-fiftieth of the beam thickness.

4.3 The test specimen sizes and fixtures for rectangular beam test specimens should be in accordance with Test Method C1161, which provides a balance between practical configurations and resulting errors, as discussed in Refs 4.4 The SCG parameters (n and D) are determined by fitting the measured experimental data to a mathematical relationship between strength and applied stress rate, log σ_f = 1/(Note 3: There are various other forms of crack velocity laws which are usually more complex or less convenient mathematically, or both, but may be physically more realistic (6). It is generally accepted that actual data cannot reliably distinguish between the various formulations. Therefore, the mathematical analysis in this test method does not cover such alternative crack velocity formulations.

4.5 The mathematical relationship between strength and stress rate was derived based on the assumption that the slow crack growth parameter is at least n ≥ 5 4.6 The mathematical analysis of test results in accordance with the method in 4.4 assumes that the material displays no rising 4.7 Slow crack growth behavior of ceramic materials exposed to stress-corrosive gases or liquid environments can vary as a function of mechanical, material, and electrochemical variables. Therefore, it is essential that test results accurately reflect the effects of specific variables under study. Only then can data be compared from one investigation to another on a valid basis or serve as a valid basis for characterizing materials and assessing structural behavior.

4.8 The strength of advanced ceramics is probabilistic in nature. Therefore, SCG that is determined from the strengths of a ceramic material is also a probabilistic phenomenon. Hence, a proper range and number of applied stress rates in conjunction with an appropriate number of specimens at each applied stress rate are required for statistical reproducibility and design Note 4: For a given ceramic material/environment system, the SCG parameter 4.9 The strength of a ceramic material for a given specimen and test fixture configuration is dependent on its inherent resistance to fracture, the presence of flaws, and environmental effects. Analysis of a fracture surface, fractography, though beyond the scope of this test method, is highly recommended for all purposes, especially to verify the mechanism(s) associated with failure (refer to Practice C1322).

4.10 The conventional analysis of constant stress-rate testing is based on a critical assumption that stress is uniform throughout the test piece. This is most easily achieved in direct tension test specimens. Only test specimens that fracture in the inner gauge section in four-point testing should be used. Three-point flexure shall not be used. Breakages between the outer and inner fixture contact points should be discounted. The same requirement applies to biaxial disk strength testing. Only fractures which occur in the inner loading circle should be used. Furthermore, it is assumed that the fracture origins are near to the tensile surface and do not grow very large relative to the thickness of rectangular beam flexure or disk strength test specimens.

4.11 The conventional analysis of constant stress-rate testing is also based on a critical assumption that the same type flaw controls strength in all specimens at all loading rates. If the flaw distribution is multimodal, then the conventional analysis in this standard may produce erroneous slow crack growth parameter estimates.

1.1 This test method covers the determination of slow crack growth (SCG) parameters of advanced ceramics by using constant stress-rate rectangular beam flexural testing, or ring-on-ring biaxial disk flexural testing, or direct tensile strength, in which strength is determined as a function of applied stress rate in a given environment at ambient temperature. The strength degradation exhibited with decreasing applied stress rate in a specified environment is the basis of this test method which enables the evaluation of slow crack growth parameters of a material.

1.2 Values expressed in this test method are in accordance with the International System of Units (SI) and IEEE/ASTM SI 10.

1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.