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ASTM E415-17

Standard Test Method for Analysis of Carbon and Low-Alloy Steel by Spark Atomic Emission Spectrometry

NORMA vydaná dňa 15.5.2017

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Informácie o norme:

Označenie normy: ASTM E415-17
Poznámka: NEPLATNÁ
Dátum vydania normy: 15.5.2017
Kód tovaru: NS-686251
Počet strán: 11
Približná hmotnosť: 33 g (0.07 libier)
Krajina: Americká technická norma
Kategória: Technické normy ASTM

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Keywords:
carbon steel, low-alloy steel, spark atomic emission, spectrometric analysis, spectrometry,, ICS Number Code 77.080.20 (Steels)

Doplňujúce informácie

Significance and Use

5.1 This test method for the spectrometric analysis of metals and alloys is primarily intended to test such materials for compliance with compositional specifications. It is assumed that all who use this test method will be analysts capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in a properly equipped laboratory.

1. Scope

1.1 This test method covers the simultaneous determination of 21 alloying and residual elements in carbon and low-alloy steels by spark atomic emission vacuum spectrometry in the mass fraction ranges shown Note 1.

Element

Composition Range, %

Applicable Range,
Mass Fraction %^A

Quantitative Range,
Mass Fraction %^B

Aluminum

0 to 0.093

0.006 to 0.093

Antimony

0 to 0.027

0.006 to 0.027

Arsenic

0 to 0.1

0.003 to 0.1

Boron

0 to 0.007

0.0004 to 0.007

Calcium

0 to 0.003

0.002 to 0.003

Carbon

0 to 1.1

0.02 to 1.1

Chromium

0 to 8.2

0.007 to 8.14

Cobalt

0 to 0.20

0.006 to 0.20

Copper

0 to 0.5

0.006 to 0.5

Manganese

0 to 2.0

0.03 to 2.0

Molybdenum

0 to 1.3

0.007 to 1.3

Nickel

0 to 5.0

0.006 to 5.0

Niobium

0 to 0.12

0.003 to 0.12

Nitrogen

0 to 0.015

0.01 to 0.055

Phosphorous

0 to 0.085

0.006 to 0.085

Silicon

0 to 1.54

0.02 to 1.54

Sulfur

0 to 0.055

0.001 to 0.055

Tin

0 to 0.061

0.005 to 0.061

Titanium

0 to 0.2

0.001 to 0.2

Vanadium

0 to 0.3

0.003 to 0.3

Zirconium

0 to 0.05

0.01 to 0.05

Note 1: The mass fraction ranges of the elements listed have been established through cooperative testing2 of reference materials.

1.2 This test method covers analysis of specimens having a diameter adequate to overlap and seal the bore of the spark stand opening. The specimen thickness can vary significantly according to the design of the spectrometer stand, but a thickness between 10 mm and 38 mm has been found to be most practical.

1.3 This test method covers the routine control analysis in iron and steelmaking operations and the analysis of processed material. It is designed for chill-cast, rolled, and forged specimens. Better performance is expected when reference materials and specimens are of similar metallurgical condition and composition. However, it is not required for all applications of this standard.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

2. Referenced Documents

E350-23	Standard Test Methods for Chemical Analysis of Carbon Steel, Low-Alloy Steel, Silicon Electrical Steel, Ingot Iron, and Wrought Iron
E406-19	Standard Practice for Using Controlled Atmospheres in Atomic Emission Spectrometry
E1019-18	Standard Test Methods for Determination of Carbon, Sulfur, Nitrogen, and Oxygen in Steel, Iron, Nickel, and Cobalt Alloys by Various Combustion and Inert Gas Fusion Techniques
E29-22	Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
E1601-19	Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method
E1329-10	Standard Practice for Verification and Use of Control Charts in Spectrochemical Analysis (Withdrawn 2019)
ASTM MNL 7	Manual on Presentation of Data and Control Chart Analysis ASTM Manual Series, ASTM International, 8th edition, 2010.
E135-23a	Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials (Includes all amendments and changes 7/17/2023).
E1763-06	Standard Guide for Interpretation and Use of Results from Interlaboratory Testing of Chemical Analysis Methods (Withdrawn 2015)
E1806-23	Standard Practice for Sampling Steel and Iron for Determination of Chemical Composition
E1950-17	Standard Practice for Reporting Results from Methods of Chemical Analysis (Withdrawn 2023)
E2972-15(2019)	Standard Guide for Production, Testing, and Value Assignment of In-House Reference Materials for Metals, Ores, and Other Related Materials
E305-21	Standard Practice for Establishing and Controlling Spark Atomic Emission Spectrochemical Analytical Curves

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