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ASTM D5175-91(2017)e1
Standard Test Method for Organohalide Pesticides and Polychlorinated Biphenyls in Water by Microextraction and Gas Chromatography (Includes all amendments And changes 4/29/2024).
NORMA vydaná dňa 15.12.2017
Informácie o norme:
Označenie normy: ASTM D5175-91(2017)e1
Poznámka: NEPLATNÁ
Dátum vydania normy: 15.12.2017
Kód tovaru: NS-804671
Počet strán: 12
Približná hmotnosť: 36 g (0.08 libier)
Krajina: Americká technická norma
Kategória: Technické normy ASTM
Kategórie - podobné normy:
Anotácia textu normy ASTM D5175-91(2017)e1 :
Keywords:
gas chromatography, microextraction, organochlorine pesticides, polychlorinated biphenyls (PCBs),, ICS Number Code 13.060.50 (Examination of water for chemical substances)
Doplňujúce informácie
| Significance and Use | |||||||||||||||||||||||||||||||||||||||||||||||||||||||||
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5.1 The extensive and widespread use of organochlorine pesticides and PCBs has resulted in their presence in all parts of the environment. These compounds are persistent and may have adverse effects on the environment. Thus, there is a need to identify and quantitate these compounds in water samples. |
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| 1. Scope | |||||||||||||||||||||||||||||||||||||||||||||||||||||||||
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1.1 This test method (1-3)2 is applicable to the determination of the following analytes in finished drinking water, drinking water during intermediate stages of treatment, and the raw source water:
1.2 Detection limits for most test method
analytes are less than 1 μg/L. Actual detection limits are highly
dependent on the characteristics of the sample matrix and the gas
chromatography system. Table
1 contains the applicable concentration range for the
precision and bias statements. Only Aroclor 1016 and 1254 were
included in the interlaboratory test used to derive the precision
and bias statements. Data for other PCB products are likely to be
similar.
1.3 Chlordane, toxaphene, and Aroclor
products (polychlorinated biphenyls) are multicomponent materials.
Precision and bias statements reflect recovery of these materials
dosed into water samples. The precision and bias statements may not
apply to environmentally altered materials or to samples containing
complex mixtures of polychlorinated biphenyls (PCBs) and
organochlorine pesticides.
1.4 For compounds other than those listed in 1.1 or for other sample sources, the analyst must demonstrate the applicability of this test method by collecting precision and bias data on spiked samples (groundwater, tap water) 1.5 This test method is restricted to use by or under the supervision of analysts experienced in the use of GC and in the interpretation of gas chromatograms. Each analyst must demonstrate the ability to generate acceptable results using the procedure described in Section 13. 1.6 Analytes that are not separated chromatographically, (analytes that have very similar retention times) cannot be individually identified and measured in the same calibration mixture or water sample unless an alternative technique for identification and quantitation exists (see 13.4). 1.7 When this test method is used to analyze unfamiliar samples for any or all of the analytes listed in 1.1, analyte identifications and concentrations should be confirmed by at least one additional technique. 1.8 The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to inch-pound units that are provided for information only and are not considered standard. 1.9 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.10 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. |
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| 2. Referenced Documents | |||||||||||||||||||||||||||||||||||||||||||||||||||||||||
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